Potassium Hydroxide → 2-Pyridinecarboxylic acid, potassium salt (1:1)

HRID 1441763ノート

反応式

HRID 1441763 の反応式
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3](C([O-])=O)[C:2]=1[C:10]([O-:12])=[O:11].[OH-].[K+:14]>CO>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:10]([O-:12])=[O:11].[K+:14]

参加物

4

反応物 2

HCID 14797Potassium HydroxideHCID 5460301HCID 5460301、化合物

生成物 1

HCID 236723372-Pyridinecarboxylic acid, potassium salt (1:1)

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

The pyridinedicarboxylate 30 (19.5 g, 0.1 mol) was treated with solid KOH (6.51 g, 0.1 mol) in 300 mL of methanol at room temperature for 2 h, giving rise to a thick pale white suspension, which was filtered and dried to provide the mono-potassium pyridinecarboxylate 3 in quantitative yield.

後処理

  1. customgiving rise to a thick pale white suspension, which
  2. filtrationwas filtered
  3. customdried

出典と根拠

ORDレコード
ord-bc670377a3164a08a96129dbab32b661
出典データセット
uspto-grants-2010_02
特許番号
US07655699B1

反応ノート

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