[1,1'-Biphenyl]-3-carbonitrile → 2-[(1,1'-Biphenyl)-3-yl]-1,2,4-triazolo[5,1-a]isoquinoline
反応式
[NH2:1][N:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]1=O.[C:13]1([C:19]2[CH:20]=[C:21]([CH:24]=[CH:25][CH:26]=2)[C:22]#[N:23])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C(OCC)(=O)C>[C:19]1([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:26]=[CH:25][CH:24]=[C:21]([C:22]2[N:23]=[C:3]3[C:4]4[C:9]([CH:10]=[CH:11][N:2]3[N:1]=2)=[CH:8][CH:7]=[CH:6][CH:5]=4)[CH:20]=1参加物
4
実験手順
This compound was prepared according to the procedure of the foregoing Example, starting from 2-amino-isoquinoline-1(2H)-one and 3-phenyl-benzonitrile. Yield 49%. M.p. 167°-69° C. (from ethyl acetate).
後処理
- customThis compound was prepared
出典と根拠
- ORDレコード
- ord-6d1772bc69df4fcaa42033a5f630f922
- 出典データセット
- uspto-grants-1982_02
- 特許番号
- US04313950
反応ノート
読み込み中…