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Peracetic Acid → Phenyl acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Peracetic Acid | HCID 6585 | — |
| 反応物 | Triphenyltin hydroxide acetate | HCID 9909408 | — |
| 反応物 | Phenylmercuric Acetate | HCID 16682730 | — |
| 生成物 | Phenyl acetate | HCID 31229 | 58% |
反応手順
The procedure of Example 1 is repeated except that 5 mmols of triphenyl tin acetate are employed instead of the phenyl mercuric acetate of Example 1, and 30 mmols of peracetic acid is used. After 4 hours of reaction at 75° C. there is obtained phenyl acetate in a yield of about 58%, and in a selectivity of about 68%, at a triphenyl tin acetate conversion of about 85%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04316045 |
| 出典データセット | uspto-grants-1982_02 |
| ORD ID | ord-bcd2cb51e5d4489f8c3c5766013152bd |
| 出典メモ | uspto-grants-1982_02 |