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Phenylmercuric Acetate → Phenyl acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phenylmercuric Acetate | HCID 16682730 | — |
| 反応物 | Phenyl iodoso diacetate | HCID 86738254 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Phenyl acetate | HCID 31229 | — |
反応手順
The procedure of Example 3 is repeated except that only 10 ml. of acetic acid is charged to the reaction vessel, thereby increasing the concentration of the phenyl mercuric acetate and phenyl iodoso diacetate reactants in the liquid. At the end of the 0.25 hour of reaction at 120° C., phenyl acetate yield is found to be increased to 68%, at a phenyl mercuric acetate conversion of about 72% and a phenyl acetate selectivity of about 94%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04316046 |
| 出典データセット | uspto-grants-1982_02 |
| ORD ID | ord-a28dddae7f5f4de8b751370c240c3100 |
| 出典メモ | uspto-grants-1982_02 |