Allylamine → HCID 20383071、化合物

反応式

[CH:1]1([C:7]2[CH:8]=[CH:9][C:10]3[O:15][CH:14]([C:16]([OH:18])=O)[CH2:13][CH2:12][C:11]=3[CH:19]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH2:20]([NH2:23])[CH:21]=[CH2:22]>>[CH:1]1([C:7]2[CH:8]=[CH:9][C:10]3[O:15][CH:14]([C:16]([NH:23][CH2:20][CH:21]=[CH2:22])=[O:18])[CH2:13][CH2:12][C:11]=3[CH:19]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

参加物

反応物 2

HCID 7853Allylamine

HCID 30170556-Cyclohexyl-3,4-dihydro-2H-1-benzopyran-2-carboxylic acid

生成物 1

HCID 20383071HCID 20383071、化合物

実験手順

5 Also was prepared, as white crystals, mp: 93°-94° C., by the procedure described in the last paragraph of Example 2, from the ethyl ester of 6-cyclohexyl-3,4-dihydro-2H-1-benzopyran-2-carboxylic acid (Witiak et al. (1975)) and 2-propenamine.

後処理

custom5 Also was prepared, as white crystals, mp: 93°-94° C., by the procedure

出典と根拠

ORDレコード: ord-37eb3bac8b1e4a5fb5e1003541a75e6b
出典データセット: uspto-grants-1979_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04178380

反応ノート

読み込み中…

参加物