戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1447849作成日:2026年10月25日

3-(Dimethylamino)-1-phenyl-2-propen-1-one → 7-Phenylpyrazolo[1,5-a]pyrimidine-3-carbonitrile

https://huagongshe.com/reaction/1447849

反応式

関与物質

役割名称HCID仕込み量
反応物3-(Dimethylamino)-1-phenyl-2-propen-1-oneHCID 353460—
反応物HCID 178510443HCID 178510443—
溶媒Acetic AcidHCID 176—
生成物7-Phenylpyrazolo[1,5-a]pyrimidine-3-carbonitrileHCID 1480415—

反応手順

A reaction mixture comprising 4.32 g. of 3-aminopyrazole-4-carbonitrile, 7.0 g. of 3-dimethylaminoacrylophenone and 25 ml. of glacial acetic acid is refluxed for 7 hours. The mixture is evaporated and the residue is treated as described in Example 1, giving the desired product, m.p. 230°-232° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04178449
出典データセットuspto-grants-1979_12
ORD IDord-58c02f12bb92434991229ab5917502a7
出典メモuspto-grants-1979_12