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Bromotriphenylmethane → 1-Bromo-5,5-dimethyl-3-triphenylmethoxy-trans-1-octene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromotriphenylmethane | HCID 11692 | — |
| 反応物 | 1-Bromo-5,5-dimethyl-trans-1-octen-3-ol | HCID 20465750 | — |
| 生成物 | 1-Bromo-5,5-dimethyl-3-triphenylmethoxy-trans-1-octene | HCID 20465692 | — |
反応手順
Treatment of 3.53 g. (15 moles) of 1-bromo-5,5-dimethyl-trans-1-octen-3-ol (Example 1177) with 4.83 g. (15 moles) of triphenylmethyl bromide in 35 ml. of pyridine and purification on Florisil®, all as described in Example 728 gives the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04179574 |
| 出典データセット | uspto-grants-1979_12 |
| ORD ID | ord-91d31985975544c7ae96496dc862002c |
| 出典メモ | uspto-grants-1979_12 |