関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Ethylhexanol | HCID 7720 | — |
| 反応物 | Ethyl (2-methylacryloyl)carbamate | HCID 13628540 | — |
| 触媒 | Hydroquinone | HCID 785 | — |
| 生成物 | 2-ethylhexyl N-methacryloylcarbamate | HCID 19973683 | 72.2% |
反応手順
A reaction vessel was charged with 15.7 g of ethyl N-methacryloylcarbamate and 52 g of 2-ethylhexyl alcohol, to which 0.1 g of hydroquinone was added and heated at 120° C. for one hour. The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 17.4 g of 2-ethylhexyl N-methacryloylcarbamate having a viscosity of 800 cp.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05606096 |
|---|
| 出典データセット | uspto-grants-1997_02 |
|---|
| ORD ID | ord-db2484a96fec493cb3de5b738a92ebcb |
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| 出典メモ | uspto-grants-1997_02 |
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