戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1452823作成日:2026年10月27日

1,1,3,3,3-Pentafluoro-1,2,2-trichloropropane → 1,1,3,3,3-Pentafluoro-1,2,2-trichloropropane

https://huagongshe.com/reaction/1452823

反応式

関与物質

役割名称HCID仕込み量
反応物1,1,3,3,3-Pentafluoro-1,2,2-trichloropropaneHCID 15335—
反応物HCID 178418361HCID 178418361—
触媒PalladiumHCID 23938—
生成物1,1,3,3,3-Pentafluoro-1,2,2-trichloropropaneHCID 15335—
生成物1,1,3,3,3-PentafluoropropeneHCID 69647—
生成物2-Chloro-1,1,3,3,3-pentafluoropropeneHCID 102335—

反応手順

The test procedure described in Example 2 was repeated except that the catalyst was 0.5% Pd on alumina, the reaction temperature was held to approximately 150° C. and the duration of the test was approximately 12.6 hours. The mole ratio of hydrogen to CF3CCl2CF2Cl introduced into the quartz reactor was approximately 1.09. The reaction product was collected and its composition was determined. The reaction resulted in a conversion of CF3CCl2CF2Cl of about 97.8%, with a selectivity for CF3CH═CF2 of 6.8%, for CF3CCl═CF2 of 85.4%, and for CF3CHClCF2Cl of 3.8%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07473810B1
出典データセットuspto-grants-2009_01
ORD IDord-9c1f5536aa5a4b74831899f17f28734d
出典メモuspto-grants-2009_01