3,4-Dimethylbenzoic acid → 3,4-dimethyl-N-(5-methylhexan-3-yl)benzamide

関与物質

役割	名称	HCID	仕込み量
反応物	3,4-Dimethylbenzoic acid	HCID 12073	—
反応物	5-Methylhexan-3-amine	HCID 22955496	—
生成物	3,4-dimethyl-N-(5-methylhexan-3-yl)benzamide	HCID 57527902	—

反応手順

Prepared in a similar manner to example 4 using 3,4-dimethylbenzoic acid and 5-methylhexan-3-amine (example 5a). 1H NMR (500 MHz, CDCl3): δ 0.94 (m, 9H); 1.38 (m, 2H); 1.46 (m, 1H); 1.65 (m, 2H); 2.29 (s, 3H); 2.30 (s, 3H); 4.18 (m, 1H); 5.70 (d, 1H); 7.17 (d, 1H); 7.46 (d, 1H); 7.55 (s, 1H). MS (248, M+H).

情報源と証拠

DOI	10.6084/m9.figshare.5104873.v1
特許番号	US07476399B2
出典データセット	uspto-grants-2009_01
ORD ID	ord-6cfe2c2000484a17823b88dae33d8fff
出典メモ	uspto-grants-2009_01