5,6,11,12-Tetrahydrodibenzo[b,f]azocine → 5-(4-Benzoylbenzoyl)5,6,11,12-tetrahydrodibenz[b,f]azocine
反応式
[CH:1]1[C:12]2[CH2:11][CH2:10][C:9]3[CH:13]=[CH:14][CH:15]=[CH:16][C:8]=3[CH2:7][NH:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:17]([C:25]1[CH:33]=[CH:32][C:28]([C:29](Cl)=[O:30])=[CH:27][CH:26]=1)(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:17]([C:25]1[CH:26]=[CH:27][C:28]([C:29]([N:6]2[CH2:7][C:8]3[CH:16]=[CH:15][CH:14]=[CH:13][C:9]=3[CH2:10][CH2:11][C:12]3[CH:1]=[CH:2][CH:3]=[CH:4][C:5]2=3)=[O:30])=[CH:32][CH:33]=1)(=[O:24])[C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1参加物
3
実験手順
As described for Example 26, 5,6,11,12-tetrahydrodibenz[b,f]azocine is reacted with 4-(benzoyl)benzoyl chloride to give the product as a solid, m.p. 89°-92° C., Mass spectrum (CI), 418(MH+)
出典と根拠
- ORDレコード
- ord-c9a5cdd9c26b4fb9a0058762ffedecd9
- 出典データセット
- uspto-grants-1998_12
- 特許番号
- US05849735
反応ノート
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