4-Propylpyridin-2-amine → HCID 178476207、化合物

HRID 1459270ノート

反応式

HRID 1459270 の反応式
[C:1]([OH:4])(=[O:3])[CH3:2].N=C1CC(C)CCN1.[NH2:13][C:14]1[CH:19]=[C:18]([CH2:20][CH2:21][CH3:22])[CH:17]=[CH:16][N:15]=1>>[C:1]([OH:4])(=[O:3])[CH3:2].[NH:13]=[C:14]1[CH2:19][CH:18]([CH2:20][CH2:21][CH3:22])[CH2:17][CH2:16][NH:15]1

参加物

3

反応物 2

HCID 70225944-Propylpyridin-2-amineHCID 1784758702-Imino-4-methylpiperidine acetate

生成物 1

HCID 178476207HCID 178476207、化合物

実験手順

The method of preparation of 2-imino-4-methylpiperidine acetate was used to convert 2-amino-4-(n-propyl)pyridine to the title compound except platinum oxide was used as the catalyst. Product was triturated with EtOAc to give a white solid. The analysis of the product was found to be consistent with the proposed structure. MH+141; 1H NMR (D2O): δ3.35-3.05 (m, 2H); 2.60-2.40 (m, 1H); 2.15-2.00 (m, 1H); 1.80-1.60 (m, 2H); 1.78 (s, 3H); 1.35-1.05 (m, 5H); 075-0.65 (m, 3H).

出典と根拠

ORDレコード
ord-302311222e864ee5bbd47375c85f2f3e
出典データセット
uspto-grants-1998_12
特許番号
US05854234

反応ノート

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