Water → Glycidoxypropyl Silanol

HRID 1461093

反応式

HRID 1461093 の反応式
O.[CH2:2]([O:6][CH2:7][CH2:8][CH2:9][Si:10](OCC)(OCC)[O:11]CC)[CH:3]1[O:5][CH2:4]1>C(O)(=O)C>[CH2:2]([O:6][CH2:7][CH2:8][CH2:9][SiH2:10][OH:11])[CH:3]1[O:5][CH2:4]1

参加物

4

反応物 2

HCID 962WaterHCID 102856gamma-Glycidoxypropyltriethoxysilane

生成物 1

HCID 123537430Glycidoxypropyl Silanol

試薬・触媒・溶媒 1

HCID 176Acetic Acid溶媒

反応条件

温度
90 °C

実験手順

In a three-necked flask equipped with a stirrer, dropping funnel and reflux condenser, 500 g water were adjusted with dilute acetic acid to a pH value of 4 to 4.5. 15 g glycidoxypropyl triethoxysilane were then added dropwise, the mixture being heated to 90° C. This temperature was maintained for 1 hour.

後処理

  1. customIn a three-necked flask equipped with a stirrer
  2. temperaturereflux condenser
  3. temperatureThis temperature was maintained for 1 hour

出典と根拠

ORDレコード
ord-c4d35faa540c401f800b316ffa07cf99
出典データセット
uspto-grants-1991_12
特許番号
US05073588

関連ノート

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