5,6-Dihydroquinoline → 5,6,7,8-Tetrahydro-7-dimethylaminoquinoline
反応式
[Cl-].[CH3:2][NH2+:3][CH3:4].[N:5]1[C:14]2[CH:13]=[CH:12][CH2:11][CH2:10][C:9]=2[CH:8]=[CH:7][CH:6]=1>>[CH3:2][N:3]([CH3:4])[CH:12]1[CH2:13][C:14]2[N:5]=[CH:6][CH:7]=[CH:8][C:9]=2[CH2:10][CH2:11]1参加物
3
実験手順
This compound was prepared from dimethylammonium chloride (1.63 g, 20 mmol) and 5,6-dihydroquinoline (1.31 g, 10 mmol) using the experimental and purification method describes in Example 48. The product (0.72 g) was an oil which was identical to the compound isolated in Example 3.
後処理
- custompurification method
出典と根拠
- ORDレコード
- ord-8cf27b10e2d64258a70bc63b4b0d63ed
- 出典データセット
- uspto-grants-1991_12
- 特許番号
- US05075303
反応ノート
読み込み中…