化工社化工社 化学情報印刷レポート · 研究参考用
2,6-Difluorobenzoyl isocyanate → Teflubenzuron
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Difluorobenzoyl isocyanate | HCID 2733369 | — |
| 反応物 | 3,5-Dichloro-2,4-difluorobenzenamine | HCID 2774000 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Teflubenzuron | HCID 91734 | — |
反応手順
Three grams (0.016 mol) of 2,6-difluoro-benzoyl isocyanate were added to a solution of 2.95 gm (0.015 mol) of 2,4-difluoro-3,5-dichloroaniline in 50 ml of toluene. The solution thus obtained was stirred for 15 hours at room temperature. Thereafter, the product which precipitated during that time was removed by suction filtration and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04457943 |
| 出典データセット | uspto-grants-1984_07 |
| ORD ID | ord-9bf4f69978b74406ae77f12ebb41fc96 |
| 出典メモ | uspto-grants-1984_07 |