HCID 12595613、化合物 → HCID 12595637、化合物
反応式
C1O[C:4]2([CH2:9][CH2:8][C:7]([N:15]([CH3:17])[CH3:16])([C:10]3[S:11][CH:12]=[CH:13][CH:14]=3)[CH2:6][CH2:5]2)[O:3]C1.ClC1C=CC(C2(N(C)C)CCC(=O)CC2)=CC=1>>[CH3:16][N:15]([CH3:17])[C:7]1([C:10]2[S:11][CH:12]=[CH:13][CH:14]=2)[CH2:8][CH2:9][C:4](=[O:3])[CH2:5][CH2:6]1参加物
3
実験手順
Following the procedure of Example 2, but substituting the appropriate quantity of 4-dimethylamino-4-(2-thienyl)cyclohexanone ethylene ketal (prepared above in Example 27H) for the 4-(p-chlorophenyl)-4-dimethylaminocyclohexanone, ethylene ketal hydrochloride there is prepared (after recrystallization from methanol-water) the title compound in 64% yield, m.p. 102°-103° C.
後処理
- customis prepared
- custom(after recrystallization from methanol-water) the title compound in 64% yield, m.p. 102°-103° C.
出典と根拠
- ORDレコード
- ord-1c007f3a120c46479d3943664de3e25b
- 出典データセット
- uspto-grants-1984_07
- 特許番号
- US04460604
反応ノート
読み込み中…