1,8-Dibromododecane → 12-Bromododecylphthalimide
反応式
[C:1]1(=[O:11])[NH:5][C:4](=[O:6])[C:3]2=[CH:7][CH:8]=[CH:9][CH:10]=[C:2]12.[K].[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH:21](Br)[CH2:22][CH2:23][CH2:24][CH3:25]>CN(C)C=O>[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][C:10]1[CH:9]=[CH:8][CH:7]=[C:3]2[C:4]([NH:5][C:1](=[O:11])[C:2]=12)=[O:6]参加物
4
実験手順
Potassium phthalimide (1 g; 5.4 mmoles) was added to a solution of 1,8-dibromododecane (5.31 g; 16.2 mmoles) in dimethylformamide (8 ml) and heated to 80° C. approx. under stirring. Reaction times and process as per Example 4.
後処理
- temperatureheated to 80° C. approx.
- customReaction times and process as per Example 4
出典と根拠
- ORDレコード
- ord-2b1425fe22a64dcf83200dc045951830
- 出典データセット
- uspto-grants-1994_04
- 特許番号
- US05302593
反応ノート
読み込み中…