Hydrazine → 8-Pyrrolidinyloctylamine

HRID 1463822ノート

反応式

HRID 1463822 の反応式
[NH2:1]N.[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7]1

参加物

4

反応物 2

HCID 9321HydrazineHCID 542934218-Pyrrolidinyloctylphthalimide

生成物 1

HCID 199335008-Pyrrolidinyloctylamine

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-pyrrolidinyloctylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

後処理

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

出典と根拠

ORDレコード
ord-8b4d10a573ec41db9f7b3f9c763bc267
出典データセット
uspto-grants-1994_04
特許番号
US05302593

反応ノート

読み込み中…