Potassium Hydroxide → 4-Methylthio-2-biphenylylcyanamide
反応式
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[C:5]([NH:15][C:16]([NH2:18])=S)[CH:4]=1.[OH-].[K+].O.O.O.C([O-])(=O)C.[Pb+2].C([O-])(=O)C>O>[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[C:5]([NH:15][C:16]#[N:18])[CH:4]=1参加物
5
実験手順
A mixture of N-(4-methylthio-2-biphenylyl)thiourea (9.6 g), potassium hydroxide (8.5 g), lead acetate trihydrate (12.5 g) and water (165 ml) was heated at 90°-95° C. for 30 minutes to give 4-methylthio-2-biphenylylcyanamide.
後処理
- temperaturewas heated at 90°-95° C. for 30 minutes
出典と根拠
- ORDレコード
- ord-8912914b9c024cf7b1e2f4aef4b2905a
- 出典データセット
- uspto-grants-1994_04
- 特許番号
- US05302720
反応ノート
読み込み中…