化工社化工社 化学情報印刷レポート · 研究参考用
Isoamyl Nitrite → 2-Methyl-4-nitrosoresorcinol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isoamyl Nitrite | HCID 8053 | — |
| 反応物 | 2-Methylresorcinol | HCID 11843 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-Methyl-4-nitrosoresorcinol | HCID 100616 | — |
反応手順
19.8 g. 2-Methylresorcinol and 13.4 g. potassium hydroxide are dissolved in 120 ml. ethanol and cooled to 5° C. 24 ml. Isopentyl nitrite are added dropwise thereto, the reaction mixture is stirred for 3 hours and the precipitate is filtered off with suction. The yellow solid material is stirred into 200 ml. 5N sulphuric acid, the bright yellow product thereby precipitating out. Yield 22 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05304645 |
| 出典データセット | uspto-grants-1994_04 |
| ORD ID | ord-63c2a46ced484bca92e3fbc8bb0f2b1c |
| 出典メモ | uspto-grants-1994_04 |