化工社化工社 化学情報印刷レポート · 研究参考用
Methyl behenate → Potassium Behenate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl behenate | HCID 13584 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Potassium Behenate | HCID 23663647 | — |
反応手順
Methyl behenate (0.375 moles/mole of sucrose to be used in Step B) is saponified by stirring at reflux in methanol containing an equivalent amount of KOH. The reaction is stirred with heating until all methyl ester has been converted to soap as indicated by infrared analysis. The soap solution is used, as is in the next reaction step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05306516 |
| 出典データセット | uspto-grants-1994_04 |
| ORD ID | ord-62e11f735d0a4f1fb83b37c1ceb0ca82 |
| 出典メモ | uspto-grants-1994_04 |