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Hydrofluoric Acid → 2-Fluoro-m-xylene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrofluoric Acid | HCID 14917 | — |
| 反応物 | 2,6-Dimethylphenyl carbonochloridate | HCID 271618 | — |
| 生成物 | 2-Fluoro-m-xylene | HCID 123065 | 51% |
反応手順
1000 ml of anhydrous hydrogen fluoride were placed at 0° C. in a stainless steel laboratory autoclave and 500 g of 2,6-dimethylphenyl chloroformate were added dropwise. The reaction was carried out and the reaction mixture worked up as described in Example 9. 2,6-Dimethylfluorobenzene was obtained in a yield of 51%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05306849 |
| 出典データセット | uspto-grants-1994_04 |
| ORD ID | ord-815b8636b4344f7db94ab8dea359cbc5 |
| 出典メモ | uspto-grants-1994_04 |