関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Antimony pentafluoride | HCID 24557 | — |
| 反応物 | 2,6-Dimethylphenylfluoroformate | HCID 10844827 | — |
| 生成物 | 2-Fluoro-m-xylene | HCID 123065 | 40% |
反応手順
3.9 g of antimony pentafluoride were added to 100 g of 2,6-dimethylphenyl fluoroformate and the mixture was heated at 200° C. for 5 hours at normal pressure. The reaction mixture was then cooled and worked up as described in Example 1. 2,6-Dimethylfluorobenzene was obtained in a yield of 40%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05306849 |
|---|
| 出典データセット | uspto-grants-1994_04 |
|---|
| ORD ID | ord-baa92f8612094a66b8c28eae6b5d3051 |
|---|
| 出典メモ | uspto-grants-1994_04 |
|---|
