3-Bromopyridine → 3-(3-Bromo-phenylsulfanyl)-6-chloro-2-methyl-1-pyridin-3-yl-1H-indole

反応式

[Br:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[C:17]3[C:12](=[CH:13][C:14]([Cl:18])=[CH:15][CH:16]=3)[NH:11][C:10]=2[CH3:19])[CH:5]=[CH:6][CH:7]=1.Br[C:21]1[CH:22]=[N:23][CH:24]=[CH:25][CH:26]=1>>[Br:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[C:17]3[C:12](=[CH:13][C:14]([Cl:18])=[CH:15][CH:16]=3)[N:11]([C:21]3[CH:22]=[N:23][CH:24]=[CH:25][CH:26]=3)[C:10]=2[CH3:19])[CH:5]=[CH:6][CH:7]=1

参加物

反応物 2

HCID 122863-Bromopyridine

HCID 667653273-(3-Bromo-phenylsulfanyl)-6-chloro-2-methyl-1H-indole

生成物 1

HCID 667654873-(3-Bromo-phenylsulfanyl)-6-chloro-2-methyl-1-pyridin-3-yl-1H-indole

実験手順

Prepared according to the procedure described in Example 27, Step 1, using the following starting materials: 3-(3-bromo-phenylsulfanyl)-6-chloro-2-methyl-1H-indole and 3-bromopyridine.

後処理

customPrepared

出典と根拠

ORDレコード: ord-6b20cceb68694c6bbeebced0c066545e
出典データセット: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09000025B2

反応ノート

読み込み中…