化工社化工社 化学情報印刷レポート · 研究参考用
1-Adamantanecarbonyl chloride → Adamantane-1-carboxylic acid (3a-ethoxy-3a,4,6,6a-tetrahydro-furo[3,4-d]thiazol-2-yl)-amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| 反応物 | 3a-Ethoxy-3a,4,6,6a-tetrahydrofuro[3,4-d]thiazol-2-ylamine | HCID 67095481 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | Adamantane-1-carboxylic acid (3a-ethoxy-3a,4,6,6a-tetrahydro-furo[3,4-d]thiazol-2-yl)-amide | HCID 67095536 | — |
反応手順
The product of Example 72B, triethylamine, and adamantane-1-carbonyl chloride were processed according to the method of Example 1A to afford the title compound. MS (ESI+) m/z 351 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09006275B2 |
| 出典データセット | uspto-grants-2015_04 |
| ORD ID | ord-21694f8b3c004ea3842006d288042474 |
| 出典メモ | uspto-grants-2015_04 |