2-Bromoethyl methyl ether → 5-Methoxy-3-(2-methoxyethyl)thiazol-2(3h)-imine hydrobromide

反応式

[CH3:1][O:2][C:3]1[S:7][C:6]([NH2:8])=[N:5][CH:4]=1.[CH3:9][O:10][CH2:11][CH2:12][Br:13]>>[BrH:13].[CH3:1][O:2][C:3]1[S:7][C:6](=[NH:8])[N:5]([CH2:12][CH2:11][O:10][CH3:9])[CH:4]=1

参加物

反応物 2

HCID 809722-Bromoethyl methyl ether

HCID 203162835-Methoxy-1,3-thiazol-2-amine

生成物 1

HCID 668606505-Methoxy-3-(2-methoxyethyl)thiazol-2(3h)-imine hydrobromide

実験手順

A mixture of Example 185A and commercially available 2-bromoethyl methyl ether (Aldrich) was processed using the method described in Example 46A to afford the title compound. MS (ESI+) m/z 189 (M+H)+.

出典と根拠

ORDレコード: ord-0514449dc4b549698f55dd7162df8d5f
出典データセット: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09006275B2

反応ノート

読み込み中…