化工社化工社 化学情報印刷レポート · 研究参考用
4-Chlorobenzoylacetonitrile → HCID 178434323、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorobenzoylacetonitrile | HCID 138308 | — |
| 反応物 | HCID 178434325 | HCID 178434325 | — |
| 生成物 | HCID 178434323 | HCID 178434323 | — |
反応手順
Following the procedure described for Example 2A, the title compound was prepared using 500 mg (2.81 mmol) 6-fluoro-3-methyl-1H-indazole-5-carbaldehyde (Example 3A) and 566 mg (3.09 mmol) 3-(4-chlorophenyl)-3-oxopropanenitrile to yield 830 mg (66% of th.) of the crude product (76% purity) which was used in the next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09018234B2 |
| 出典データセット | uspto-grants-2015_04 |
| ORD ID | ord-cd03ffae62884aea9ce0b0eed8fed7ae |
| 出典メモ | uspto-grants-2015_04 |