化工社化工社 化学情報印刷レポート · 研究参考用
Manidipine → Manidipine dihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Manidipine | HCID 4008 | — |
| 反応物 | Isopropanol hydrochloride | HCID 21912024 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | Manidipine dihydrochloride | HCID 150762 | — |
反応手順
Manidipine base was dissolved in acetone (15 ml). The pH of the solution was adjusted to 1-1.5 with IPA-HCl solution with constant stifling to get manidipine Dihydrochloride. The reaction mass was filtered and dried for 2 hours (yield: 3 gm).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09018376B2 |
| 出典データセット | uspto-grants-2015_04 |
| ORD ID | ord-dc71e9cd1adf44b5ab0ed679eaacd20c |
| 出典メモ | uspto-grants-2015_04 |