(3,5-Dichlorophenyl)hydrazine monohydrochloride → 4,6-Dichloro-3,3-dimethyl-2,3-dihydro-1H-indole

HRID 1475314ノート

反応式

HRID 1475314 の反応式
Cl.[Cl:2][C:3]1[CH:4]=[C:5]([NH:10]N)[CH:6]=[C:7]([Cl:9])[CH:8]=1.ClC1C=[C:20]2[C:16]([C:17](C)(C)CN2)=[CH:15]C=1>>[Cl:2][C:3]1[CH:8]=[C:7]([Cl:9])[CH:6]=[C:5]2[C:4]=1[C:16]([CH3:20])([CH3:17])[CH2:15][NH:10]2

参加物

3

反応物 2

HCID 2723913(3,5-Dichlorophenyl)hydrazine monohydrochlorideHCID 204468746-chloro-3,3-dimethyl-2,3-dihydro-1H-indole

生成物 1

HCID 812227034,6-Dichloro-3,3-dimethyl-2,3-dihydro-1H-indole

実験手順

Prepared from 3,5-dichlorophenylhydrazine hydrochloride in an analogous manner to that described for 6-chloro-3,3-dimethyl-2,3-dihydro-1H-indole (Preparation 25). MS: [M+H]+=216.

出典と根拠

ORDレコード
ord-e8f371ad3e9a49c381a267567988e914
出典データセット
uspto-grants-2015_04
特許番号
US09018214B2

反応ノート

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