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Sulfuric Acid → 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide | HCID 71811587 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide sulfate | HCID 118387004 | 72% |
反応手順
2-amino-N-(2-methoxyphenyl)-6-(4-nitrophenyl-thio)benzamide dissolved in EA, stirred at room temperature, while dropped H2SO4 into mixture till occurred to white solid. The reaction mixture was filtered to get White solid; 72% yield;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09402819B2 |
| 出典データセット | uspto-grants-2016_08 |
| ORD ID | ord-46c5fcb07c94481a8e8f0d3a8d9e85a9 |
| 出典メモ | uspto-grants-2016_08 |