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3-Ethylamino-4-methylphenol → HCID 86680721、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Ethylamino-4-methylphenol | HCID 8428 | — |
| 反応物 | Acetic acid, 2-(4-formylphenoxy)- | HCID 89177 | — |
| 反応物 | 1-Ethyl-2,2,4-trimethyl-1,2-dihydroquinolin-7-ol | HCID 15451103 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 86680721 | HCID 86680721 | 12% |
反応手順
Dye 4 (shown below) was prepared using the procedure described in Example 4 except that 3-(ethylamino)-4-methylphenol and 2-(4-formylphenoxy)acetic acid substituted for 1-ethyl-2,2,4-trimethyl-1,2-dihydroquinolin-7-ol and 2-(4-formylphenoxy)acetic acid. Yield: 12%. λabs=525 nm (in methanol), λem=540 nm (in methanol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09416153B2 |
| 出典データセット | uspto-grants-2016_08 |
| ORD ID | ord-f2175f46161d40afa0cb5babeaf38a55 |
| 出典メモ | uspto-grants-2016_08 |