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ethyl (1R,2S)-2-phenylcyclopropane-1-carboxylate → (3-Phenylcyclopentyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | ethyl (1R,2S)-2-phenylcyclopropane-1-carboxylate | HCID 816743 | — |
| 反応物 | Methyl 3-phenylcyclopentane-1-carboxylate | HCID 14093250 | — |
| 生成物 | (3-Phenylcyclopentyl)methanol | HCID 13354127 | 86.3% |
反応手順
Instead of ethyl cis-2-phenylcyclopropanecarboxylate, 3-phenyl-cyclopentanecarboxylic acid methyl ester (1.76 g) was used and treated by the same technique as in Reference Example 23-1(2) to give (3-phenylcyclopentyl)methanol as a colorless oil (1.31 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09422240B2 |
| 出典データセット | uspto-grants-2016_08 |
| ORD ID | ord-82d2a0acb592432c81810c3a9bb3555c |
| 出典メモ | uspto-grants-2016_08 |