5-Iodo-2,4-dimethylbenzoic acid → Methyl 4-cyclopropyl-5-formyl-2-methylbenzoate
反応式
[CH:1]([C:3]1[C:4]([CH3:14])=[CH:5][C:6]([CH3:13])=[C:7]([CH:12]=1)[C:8]([O:10][CH3:11])=[O:9])=[O:2].[CH:15]1(C2C(I)=CC(C(O)=O)=C(C)C=2)C[CH2:16]1.IC1C(C)=CC(C)=C(C=1)C(O)=O>>[CH:14]1([C:4]2[C:3]([CH:1]=[O:2])=[CH:12][C:7]([C:8]([O:10][CH3:11])=[O:9])=[C:6]([CH3:13])[CH:5]=2)[CH2:16][CH2:15]1参加物
4
実験手順
The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 83.2, except 4-cyclopropyl-5-iodo-2-methylbenzoic acid (compound 86.3) was used in place of 5-iodo-2,4-dimethylbenzoic acid (compound 1.3).
出典と根拠
- ORDレコード
- ord-d3373be8ed4d497794ca74c71b162496
- 出典データセット
- uspto-grants-2016_08
- 特許番号
- US09428502B2
反応ノート
読み込み中…