tert-Butyl 4-formyl-4-methylpiperidine-1-carboxylate → HCID 178432556、化合物

反応式

[I:1][C:2]1[NH:6]C(C(C)C)=[N:4][C:3]=1[CH3:10].[CH:11]([C:13]1([CH3:26])[CH2:18][CH2:17][N:16]([C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])[CH2:15][CH2:14]1)=O>>[I:1][C:2]1[NH:6][C:11]([C:13]2([CH3:26])[CH2:18][CH2:17][N:16]([C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])[CH2:15][CH2:14]2)=[N:4][C:3]=1[CH3:10]

参加物

反応物 2

HCID 22248051tert-Butyl 4-formyl-4-methylpiperidine-1-carboxylate

HCID 178432758HCID 178432758、化合物

生成物 1

HCID 178432556HCID 178432556、化合物

実験手順

The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 159.2, except tert-butyl 4-formyl-4-methylpiperidine-1-carboxylate was used in place of isobutyraldehyde. m/z (ES+) 406 (M+H)+.

出典と根拠

ORDレコード: ord-d663e1ef8e1c4f4184289a4ab6b318a0
出典データセット: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09428502B2

反応ノート

読み込み中…