関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Boric Acid | HCID 7628 | — |
| 反応物 | Hexylene Glycol | HCID 7870 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL | HCID 352515 | — |
反応手順
61.2 g of boric acid (1 mol) and 118.2 g of 2-methyl-2,4-pentanediol (1 mol) and 200 ml of heptane are charged to a reaction flask equipped with stirrer, Marcusson apparatus and reflux condenser. The reaction mixture is heated up to its reflux temperature (about 95° C.), with stirring, and is kept at that temperature for a 4-hour period.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05370807 |
|---|
| 出典データセット | uspto-grants-1994_12 |
|---|
| ORD ID | ord-eaeb699ad1e74e04bbf19442810f1b08 |
|---|
| 出典メモ | uspto-grants-1994_12 |
|---|
