関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Isobutyronitrile | HCID 6559 | — |
| 反応物 | 2-Morpholinoaniline hydrochloride | HCID 18952284 | — |
| 生成物 | N-(2-morpholinophenyl)isobutyramidine | HCID 178449872 | — |
反応手順
A mixture of 4-(2-aminophenyl)morpholine hydrochloride (10 g) and isobutyronitrile (60 ml) was heated at 165° C. for 26 hours in a sealed stainless steel pressure vessel to yield N-(2-morpholinophenyl)isobutyramidine (m.p. 140°-141° C.) which was recrystallised from hexane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05373008 |
|---|
| 出典データセット | uspto-grants-1994_12 |
|---|
| ORD ID | ord-030dc84115224d40a2f2a3b18cc66c49 |
|---|
| 出典メモ | uspto-grants-1994_12 |
|---|
