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Salicylaldehyde → 2-dodecylthio-N-(salicylidene)aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Salicylaldehyde | HCID 6998 | — |
| 反応物 | 2-(Dodecylthio)-aniline | HCID 4670379 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-dodecylthio-N-(salicylidene)aniline | HCID 136084610 | 97.2% |
反応手順
Into a 1-liter flask equipped with condenser, stirrer and thermometer, were placed 220 g (0.75 mol of 2-(dodecylthio)aniline, 200 g of ethanol, and 91.5 g (0.75 mol) of salicylaldehyde. The resultant solution was heated at reflux overnight. Upon cooling, solvent was removed at reduced pressure to afford 290 g (97%) of product as a dark yellow/brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05376451 |
| 出典データセット | uspto-grants-1994_12 |
| ORD ID | ord-e376a7c11818497e9a92e5656d2c5768 |
| 出典メモ | uspto-grants-1994_12 |