関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzophenone oxime | HCID 11324 | — |
| 反応物 | 4-{3-[4-(1-Chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran | HCID 19379931 | — |
| 生成物 | Benzophenone | HCID 3102 | 38% |
反応手順
Using an analogous procedure to that described in Example 1 except that the reactants were heated to 60° C. for 2 hours, benzophenone oxime was reacted with 4-{3-[4-(1-chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran to give benzophenone O-}4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-α-methylbenzyl}oxime as an oil in 38% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05376680 |
|---|
| 出典データセット | uspto-grants-1994_12 |
|---|
| ORD ID | ord-2747f318a42e403aaa12914687b61a47 |
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| 出典メモ | uspto-grants-1994_12 |
|---|
