Ammonia → HCID 66554144、化合物

反応式

COCC1C=C([NH2:10])C=CC=1N.N.[N+:13]([C:16]1[CH:21]=[CH:20][C:19](Cl)=[CH:18][C:17]=1[CH2:23][O:24][CH3:25])([O-:15])=[O:14]>>[N+:13]([C:16]1[CH:21]=[CH:20][C:19]([NH2:10])=[CH:18][C:17]=1[CH2:23][O:24][CH3:25])([O-:15])=[O:14]

参加物

反応物 3

HCID 222Ammonia

HCID 97938592-Methoxymethyl-p-phenylenediamine

HCID 133378004-Chloro-2-(methoxymethyl)-1-nitrobenzene

生成物 1

HCID 66554144HCID 66554144、化合物

実験手順

Another embodiment of the present application relates to a method of making 2-methoxymethyl-1,4-benzenediamine comprising the steps: (a) introducing ammonia to a 4-nitro-3-methoxymethyl-chlorobenzene to obtain 4-nitro-3-methoxymethyl-aminobenzene; and (b) hydrogenating the 4-nitro-3-methoxymethyl-aminobenzene in the presence of a hydrogenation catalyst to obtain the 2-methoxymethyl-1,4-benzenediamine.

出典と根拠

ORDレコード: ord-119423b1a8624b24b160d3a463c9f4b4
出典データセット: uspto-grants-2015_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US09216945B2

反応ノート

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