2-Pentyl-7-vinyl-4,5-dihydronaphtho[2,1-d]thiazole → 2-Pentyl-4,5-dihydronaphtho[2,1-d]thiazole-7-carbaldehyde

HRID 1506492ノート

反応式

HRID 1506492 の反応式
C(C1C=CC(C2ON=[C:13]3[C:16]4[C:21]([CH2:22][CH2:23][C:12]=23)=[CH:20][C:19]([CH:24]=[O:25])=[CH:18][CH:17]=4)=CC=1C(F)(F)F)C(C)C.[CH2:30]([C:35]1[S:36]C2C3C(=CC(C=C)=CC=3)CCC=2[N:39]=1)[CH2:31][CH2:32][CH2:33][CH3:34]>>[CH2:30]([C:35]1[S:36][C:13]2[C:16]3[C:21](=[CH:20][C:19]([CH:24]=[O:25])=[CH:18][CH:17]=3)[CH2:22][CH2:23][C:12]=2[N:39]=1)[CH2:31][CH2:32][CH2:33][CH3:34]

参加物

3

反応物 2

HCID 671716022-Pentyl-7-vinyl-4,5-dihydronaphtho[2,1-d]thiazoleHCID 866698863-(4-Isobutyl-3-(trifluoromethyl)phenyl)-4,5-dihydronaphtho[1,2-c]isoxazole-7-carbaldehyde

生成物 1

HCID 866699272-Pentyl-4,5-dihydronaphtho[2,1-d]thiazole-7-carbaldehyde

実験手順

This compound was prepared according to the procedure described for Preparation 23D, employing 192 mgs of 2-pentyl-7-vinyl-4,5-dihydronaphtho[2,1-d]thiazole (86C). Yield: (190 mgs, 98%). LC/MS M+1=286.

後処理

  1. customThis compound was prepared

出典と根拠

ORDレコード
ord-4ee20524911e4073a65be5e5a74abf0c
出典データセット
uspto-grants-2015_12
特許番号
US09216972B2

反応ノート

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