Chlorosuccinimide → HCID 90280186、化合物
反応式
[CH:1](=[N:10][OH:11])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.C1C(=O)N([Cl:19])C(=O)C1>CN(C=O)C>[OH:11][N:10]=[C:1]([Cl:19])/[CH:2]=[CH:3]\[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1参加物
4
実験手順
To a stirred solution of cinnamaldoxime (10 g, 68 mmol) in DMF (100 mL) at room temperature was added solid NCS (9.08 g, 68 mmol). The suspension was stirred at room temperature overnight. The reaction mixture was poured into ice-water, extracted with a mixture of ethyl acetate and hexanes (7:3, 3×), dried with Na2SO4, concentrated and dried in vacuum to give the title compound.
後処理
- extractionextracted with a mixture of ethyl acetate and hexanes (7:3, 3×)
- dry with materialdried with Na2SO4
- concentrationconcentrated
- customdried in vacuum
出典と根拠
- ORDレコード
- ord-9bcfa6fa51cd4bbab05c4af939d27f79
- 出典データセット
- uspto-grants-2015_12
- 特許番号
- US09220710B2
反応ノート
読み込み中…