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HRID 1509364作成日:2026年10月26日

Water → Salvinorin B

https://huagongshe.com/reaction/1509364

反応式

関与物質

役割名称HCID仕込み量
反応物WaterHCID 962—
反応物Sodium CarbonateHCID 10340—
反応物Salvinorin AHCID 128563—
溶媒MethanolHCID 887—
生成物Salvinorin BHCID 1144068542.3%

反応手順

To a solution of Salvinorin A (500 mg, 1.15 mM) in methanol (10 ml) was added solid sodium carbonate (490 mg, 4.6 mM) and the mixture stirred at room temperature overnight. Water (20 ml) was added to mixture and the mixture stirred for 30 mins. The solution was filtered and the filter-cake washed with ice-cold water (20 ml) and ice-cold methanol (20 ml) and dried in a dessicator to give Salvinorin B (191 mg, 42%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09222949B2
出典データセットuspto-grants-2015_12
ORD IDord-fde16edeb1b248fdb5fe3b8ab8ff05a5
出典メモuspto-grants-2015_12