化工社化工社 化学情報印刷レポート · 研究参考用
Water → Salvinorin B
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Salvinorin A | HCID 128563 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Salvinorin B | HCID 11440685 | 42.3% |
反応手順
To a solution of Salvinorin A (500 mg, 1.15 mM) in methanol (10 ml) was added solid sodium carbonate (490 mg, 4.6 mM) and the mixture stirred at room temperature overnight. Water (20 ml) was added to mixture and the mixture stirred for 30 mins. The solution was filtered and the filter-cake washed with ice-cold water (20 ml) and ice-cold methanol (20 ml) and dried in a dessicator to give Salvinorin B (191 mg, 42%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09222949B2 |
| 出典データセット | uspto-grants-2015_12 |
| ORD ID | ord-fde16edeb1b248fdb5fe3b8ab8ff05a5 |
| 出典メモ | uspto-grants-2015_12 |