Hydrochloric Acid → 2-(Hydroxymethyl)-5-mercapto-4(1h)-pyridinol hydrochloride salt
反応式
C([O:4][CH2:5][C:6]1[NH:7][CH:8]=[C:9]([S:13]C(C)(C)C)[C:10](=[O:12])[CH:11]=1)(=O)C.[ClH:18]>>[ClH:18].[OH:4][CH2:5][CH:6]1[CH:11]=[C:10]([OH:12])[C:9]([SH:13])=[CH:8][NH:7]1参加物
3
反応条件
- 温度
- 80 °C
実験手順
A mixture of {5-[(1,1-dimethylethyl)thio]-4-oxo-1,4-dihydro-2-pyridinyl}methyl acetate (240 mg, 0.94 mmol) and concentrated hydrochloric acid (2 ml) was heated to 80° C. overnight. The solvent was evaporated affording a pale yellow solid.
後処理
- customThe solvent was evaporated
- customaffording a pale yellow solid
出典と根拠
- ORDレコード
- ord-9a5726d044784afe8533dfb5fa5b7ab4
- 出典データセット
- uspto-grants-2010_06
- 特許番号
- US07732460B2
反応ノート
読み込み中…