2-(Dimethylamino)ethanol → 2-(3-(benzyloxy)phenoxy)-N,N-dimethylethanamine
反応式
NC1N(C(OC(C)(C)C)=O)N=C(C2C=CC(O)=CC=2)C=1C#N.[CH3:23][N:24]([CH3:28])[CH2:25][CH2:26][OH:27].[CH2:29]([O:36][C:37]1[CH:38]=[C:39](O)[CH:40]=[CH:41][CH:42]=1)[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[CH2:29]([O:36][C:37]1[CH:42]=[C:41]([CH:40]=[CH:39][CH:38]=1)[O:27][CH2:26][CH2:25][N:24]([CH3:28])[CH3:23])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1参加物
4
実験手順
Compound 113A was prepared in a similar manner to the synthesis of step 1 of Example 35 by substituting compound 34D and compound 31F with 2-(dimethylamino)ethanol and 3-(benzyloxy)phenol, respectively: DCI (+)MS: 272 (M+H)+.
出典と根拠
- ORDレコード
- ord-e085dc17c5ac429fa2e4f8374ba75308
- 出典データセット
- uspto-grants-2012_07
- 特許番号
- US08232273B2
反応ノート
読み込み中…