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Hydrogen Bromide → (R)-3-(3,4-Dihydroxyphenyl)-2-propylamine hydrobromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 3,4-Dma, (R)- | HCID 11769408 | — |
| 生成物 | (R)-3-(3,4-Dihydroxyphenyl)-2-propylamine hydrobromide | HCID 67643451 | — |
反応手順
A solution of (R)-3-(3,4-dimethoxyphenyl)-2-propylamine hydrochloride1 (500 mg, 2.15 mMol) in hydrogen bromide (48%, 5 ml) was stirred at 100° C. under an argon atmosphere for 20 hours. After cooling, the solvent was evaporated and the residue was dried giving the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05726165 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-a3c93df638364213adea34d2adfb06d5 |
| 出典メモ | uspto-grants-1998_03 |