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3-[1,2,3]Triazol-2-yl-pyridine-2-carboxylic acid → tert-Butyl 5-(3-(2H-1,2,3-triazol-2-yl)picolinoyl)hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-[1,2,3]Triazol-2-yl-pyridine-2-carboxylic acid | HCID 66742288 | — |
| 反応物 | HCID 178451519 | HCID 178451519 | — |
| 反応物 | HCID 178524291 | HCID 178524291 | — |
| 生成物 | tert-Butyl 5-(3-(2H-1,2,3-triazol-2-yl)picolinoyl)hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate | HCID 86669169 | — |
反応手順
tert-Butyl 5-(3-(2H-1,2,3-triazol-2-yl)picolinoyl)hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate was prepared in a manner analogous to Intermediate 59 substituting 3-[1,2,3]triazol-2-yl-pyridine-2-carboxylic acid (Intermediate 72) for 2-(4H-[1,2,4]triazol-3-yl)-benzoic acid. MS (ESI) mass calculated for C19H24N6O3, 384.19; m/z found, 385.1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09079911B2 |
| 出典データセット | uspto-grants-2015_07 |
| ORD ID | ord-946c7527b05b49ebb847a39c85b16ebc |
| 出典メモ | uspto-grants-2015_07 |