HCID 178476752、化合物 → Zinc Acetate
反応式
[Zn:1](OC(C)=O)[O:2][C:3]([CH3:5])=[O:4].O.O>CO>[C:3]([O-:4])(=[O:2])[CH3:5].[Zn+2:1].[C:3]([O-:4])(=[O:2])[CH3:5]参加物
3
試薬・触媒・溶媒 1
実験手順
83.7 g of MeOH was added to Zn(OAc)2.2H2O (19.88 g) in a beaker to form 0.85 mol/L zinc acetate solution. 12.72 g of concentrated NaOH aqueous solution (49.8 wt %) was diluted with 83.7 g of MeOH followed by mixing with the Zn(OAc)2 solution under vigorous stirring. The reaction temperature of the system was maintained at 62° C. 4 minutes after the NaOH solution was mixed with the Zn(OAc)2 solution, 80 mL of 0.05 mol/L sodium oleate aqueous solution was added to the reaction solution. White precipitate formed almost immediately after the addition of sodium oleate. The reaction solution was aged at 62° C. for 45 minutes.
出典と根拠
- ORDレコード
- ord-ee568a6d4aea49a2bf4e62db318f8359
- 出典データセット
- uspto-grants-2015_07
- 特許番号
- US09090468B2
反応ノート
読み込み中…