HCID 178476752、化合物 → HCID 178476751、化合物
反応式
[Zn:1]([O:6][C:7]([CH3:9])=[O:8])[O:2][C:3]([CH3:5])=[O:4].O.O>CO>[Zn:1]([O:6][C:7]([CH3:9])=[O:8])[O:2][C:3]([CH3:5])=[O:4]参加物
3
実験手順
111.45 g of MeOH was added to Zn(OAc)2.2H2O in a 3-necked RBF to form 0.595 mol·L−1 Zn(OAc)2 methanolic solution (1.134 L). 18.43 g of KOH was dissolved in MeOH to form 1.134 L KOH solution with a concentration of 1.01 mol·L−1. The KOH solution was mixed with the Zn(OAc)2 methanolic solution under vigorous stirring in RPF. The reaction temperature of the system was maintained at 62° C. seconds after the KOH solution was mixed with the Zn(OAc)2 methanolic solution, 0.05 mol·L−1 sodium oleate aqueous solution (0.448 L) was added to the reaction solution. White precipitate formed almost immediately after the addition of sodium oleate. The reaction solution was aged at 62° C. for 10 minutes.
出典と根拠
- ORDレコード
- ord-6c4141cb2d2a457d944da11ecac9a0e3
- 出典データセット
- uspto-grants-2015_07
- 特許番号
- US09090468B2
反応ノート
読み込み中…