Melamine → 1,3,5-Triazinane-2,4,6-triimine--hydrogen chloride (1/1)

HRID 1530359ノート

反応式

HRID 1530359 の反応式
[N:1]1[C:8]([NH2:9])=[N:7][C:5]([NH2:6])=[N:4][C:2]=1[NH2:3].[ClH:10].NC(N)=O>O>[ClH:10].[N:1]1[C:8]([NH2:9])=[N:7][C:5]([NH2:6])=[N:4][C:2]=1[NH2:3]

参加物

4

反応物 2

HCID 7955Melamine3 回HCID 101721Urea hydrochloride2 回

生成物 1

HCID 5220661,3,5-Triazinane-2,4,6-triimine--hydrogen chloride (1/1)

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

16 g of melamine powder obtained from DSM (Netherlands) were added to 67 ml of water in a beaker. Following addition of the melamine powder, 18 ml of urea hydrochloric acid (Novoc ACL) was added dropwise to the beaker with stirring until the pH of the solution reached about 1.5. Addition of the urea hydrochloric acid composition solubilized the melamine powder forming a compound of Formula I (melamine hydrochloride).

後処理

  1. additionwas added dropwise to the beaker

出典と根拠

ORDレコード
ord-aeb8e47d853949849b8132f774df4997
出典データセット
uspto-grants-2015_07
特許番号
US09091019B2

反応ノート

読み込み中…