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4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)pentanoic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxybenzenethiol | HCID 12765 | — |
| 反応物 | Ethyl 2-bromovalerate | HCID 79071 | — |
| 生成物 | 2-(4-Methoxy-phenylsulfanyl)pentanoic acid ethyl ester | HCID 54570902 | — |
反応手順
2-(4-Methoxy-phenylsulfanyl)-pentanoic acid ethyl ester was prepared according to the general method as outlined in example 9. Starting from ethyl 2-bromovalerate (8.23 g, 39.3 mmol) and 4-methoxythiophenol (5 g, 35.7 mmol), 10.46 g (100%); clear oil; MS: 269 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06197791B1 |
| 出典データセット | uspto-grants-2001_03 |
| ORD ID | ord-f50452f1096b484690920df2dcdca0a3 |
| 出典メモ | uspto-grants-2001_03 |